United States

Lightweight alloys such as aluminum alloy and magnesium alloy have garnered significant attention due to their widespread use in various industries, including aerospace, automotive, and marine applications. These applications usually require excellent corrosion performance of the alloys. Laser surface treatment (LST) has emerged as a promising surface modification technique to enhance the corrosion resistance of these alloys for its automation and reproducibility. In this study, the effects of LST based on a nanosecond pulsed laser on the corrosion resistance of lightweight metal alloys, specifically AA6061 and AZ31, were studied. LST was performed underwater, using the nanosecond laser and without using a protective coating or layer on the workpiece. The corrosion behaviors of these alloys were analyzed through electrochemical tests, including open circuit potential (OCP), electrochemical impedance spectroscopy (EIS), and potentiodynamic polarization (PDP) measurements. The results demonstrated that LST significantly improved the polarization resistance, and higher laser power intensities led to increased corrosion resistance and reduced corrosion rates. This enhancement in anti-corrosion performance is attributed to the formation of a protective oxide layer on the surface, acting as a barrier against corrosion. The findings underscore the potential of laser surface treatment as a viable technique for enhancing the corrosion resistance of lightweight metal alloys.

ICALEO 2024

Enhancing Corrosion Resistance of Lightweight Metal Alloys through Laser Surface Processing

corrosion behavior

lightweight metal alloy

laser surface processing

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technical paper

#### Welcome to the 43rd annual ICALEO!

Attention laser enthusiasts, innovators, and industry leaders! Get ready to immerse yourself in the exciting world of lasers at the 43rd annual ICALEO conference. This year, we gathered in the iconic city of Hollywood, California, for cutting-edge technology, groundbreaking presentations, and unparalleled networking opportunities.
Whether you're a seasoned professional or new to the field of photonics, the 43rd annual ICALEO had something for everyone. 

#### General Chair Welcome Message

It is with immense joy and anticipation that I extend a warm welcome to each and every one of you as the General Chair of this year's ICALEO conference.

This year, we find ourselves in the iconic setting of Hollywood, serving as a fitting backdrop for the extraordinary developments in laser technology and applications unfolding in our community.

Our main sessions cover a diverse range of topics, from the intricacies of micro and nano processing to the transformative power of laser additive manufacturing. We will explore the frontiers of battery technology, delve into the intricate world of artificial intelligence, and witness the seamless integration of lasers into these realms.

For those joining us for the first time, we extend an especially heartfelt welcome. ICALEO is not just a conference; it's a convergence of minds, ideas, and innovations. Beyond the formal sessions, I encourage you to engage in informal exchanges. The spirit of discovery and camaraderie is as much a part of the ICALEO experience as the scheduled sessions.

Thank you for being a part of ICALEO 2024. Whether you are a returning participant or a first-time attendee, your presence adds immeasurable value to our vibrant community. May this conference be, this year again, a catalyst for inspiration, collaboration, and breakthroughs that will resonate in our community and beyond.

Eric Mottay 
Congress General Chair, ICALEO 2024


#### About LIA

The Laser Institute of America (LIA) is the professional society for laser applications and safety. Our mission is to foster lasers, laser applications, and laser safety worldwide. Serving the industrial, medical, research and government communities for over 50 years, LIA offers technical information, training and networking opportunities to laser users
from around the globe.

#### About LIA Conferences

The conferences of the Laser Institute of America are the town square of the laser community. A large and diverse group, laser professionals often find themselves disconnected from each other. LIA conferences, however, bring the university researcher, the business executive and the production floor user together under one roof for a unique and
rewarding networking opportunity.

#### Program Tracks
Below is the list of all tracks that were on ICALEO 2024 Conference.

##### Laser Additive Manufacturing
* The Laser Additive Manufacturing (LAM) track is a forum to explore the latest innovations and research in laser-based additive manufacturing (LAM). The Laser Additive Manufacturing track focuses on diverse topics, including laser-based powder bed fusion (PBF-LB), directed energy deposition (DED), and other emerging techniques revolutionizing modern manufacturing processes. From materials science to process optimization, from design innovation to industrial implementation, this track connects researchers, engineers, and industry leaders to exchange insights and share breakthroughs in laser additive manufacturing.

##### Laser Materials Macroprocessing
* The Macroprocessing track comprises some of the most productive laser processing applications. Although these applications have been broadly adopted, researchers and industry are persistently innovating to provide new techniques and novel technologies to advance macro materials processing. The attendees will share and discuss those exciting achievements of their research with peers in these macroscopic specialized sessions.

##### Laser Materials Microprocessing
* The Microprocessing track will consist of papers and talks featuring a wide spectrum of applications and innovative equipment for materials processing in microscales with a strong focus on processes with Short and Ultrashort Pulsed Lasers. The presentations will introduce the latest and greatest advancements in their respective fields, presented by world-leading companies and research organizations. This year we will have talks around the headlines of “Beam shaping”, “Glass”, “Surface processing” and “Drilling” between other topics.

##### Frontiers in Laser Applications
* The Frontier in Laser Applications (FLA) track explores recent, cutting-edge applications of lasers, highlighting innovation at the transition of research and industry. The track has included presentations from a variety of fields: Novel 3-D Printing, Advanced Manufacturing, Laser Manufactured Devices, and Frontiers in Laser Processing. The sessions under the Frontier in Laser Application track promise to bring diverse and unique perspectives from real-world applications across laser manufacturing.

##### Laser in Battery Manufacturing
* Electrification is crucial to address global environmental challenges. The laser plays a key role in most manufacturing steps in battery production with all possible laser applications from ablation, structuring, welding, cutting, and marking. Further improvements in the batteries’ power densities, fast charging properties, and yield in battery production are related to photonics and, thus, lasers. We will hear and discuss the latest developments in research, development, and industrial applications. Join us for this year’s Battery Track.

##### Artifical Intelligence in Laser Processing
* The track ‘Artificial Intelligence in Laser Processing’ at ICALEO 2024 explores the fusion of AI and laser manufacturing. Discover cutting-edge research on optimizing laser processes and enhancing manufacturing efficiency. Explore AI’s diverse applications in parameter optimization, quality prediction, real-time process monitoring, and control. Join us to unlock the potential of AI-driven solutions revolutionizing laser materials processing, delivering unprecedented precision, productivity, and innovation.

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Attention laser enthusiasts, innovators, and industry leaders! Get ready to immerse yourself in the exciting world of lasers at the 43rd annual ICALEO conference. 

The laser peening is a surface treatment technology that improves the mechanical performance of metals. For instance, it has been utilized to increase the resistance of a metal to crack initiation, extend the fatigue life, and enhance the fatigue strength. These effects are imparted by shockwave generated by the expansion of laser-induced ablation plasma. Utilizing double-pulse laser ablation is one of the methods to improve a coupling of the laser beam with the plasma plume and target material. With double-pulse laser ablation, a target material is irradiated by two pulsed laser beams separated by a nanosecond inter-pulse delay time. It is reported that this irradiation method allows for a more effective energy delivery to the plasma plume and target material. In this study, double-pulse laser ablation has been adopted for laser peening. The experiments were performed by two Nd: YAG Q-switched pulsed lasers (wavelength: 532 nm) in water ambient. Austenitic stainless steel SUS316L was used as the target sample. The pulse durations of the first pulse and second pulse were 6 and 4 ns, respectively. Varying the inter-pulse delay time, the surface hardness on the sample after laser peening was evaluated. The results indicated that the surface hardness depends on the inter-pulse delay time. It is found that optimizing the inter-pulse delay time for a double-pulse laser enables enhancement of the laser peening effect.

Double-Pulse Laser Peening as a Surface Enhancement Technology

Pure copper has antimicrobial effect, and the development of pure copper coating technology for product surfaces is needed to prevent the spread of infections. To achieve high antimicrobial performance in coatings, it is essential to form a coating with high copper purity and minimal defects. In this study, we attempted to form a pure copper coating layer on a SS304 substrate using multi-beam directed energy deposition with blue diode lasers. In the coating layer formation process, multiple bead layers are overlapped to form a smooth surface and two different types of joining is conducted simultaneously: the similar material joining area with the remelted previous layer, and the dissimilar material joining area with the substrate. However, it was challenging to conduct this process for SS304 and pure copper, due to their significantly different thermal properties. Therefore, we varied the hatching distance to control the heat input to both joining areas and investigated the effect on the quality of the coating layer. The results showed that there is an optimal ratio of similar and dissimilar joining areas, at which a high-quality coating layer with few voids and low dilution is formed. Furthermore, antimicrobial tests showed that the pure copper coating layer formed in this study exhibited the antimicrobial performance equivalent to those of a pure copper plate.

Pure Copper Coating by Multi Beam Directed Energy Deposition With Blue Lasers for Antimicrobial Effect

The electrification of the mobility sector is vital to meet the targets for reducing greenhouse gas emissions. Besides battery-based mobility solutions, polymer electrolyte membrane fuel cells (PEMFCs) are a promising technology for electrifying drive trains, especially in heavy-duty applications, such as maritime or logistics. Bipolar plates, a key component of PEMFCs, can consist of two stainless-steel foils that must be welded to be gas-tight. In order to join the two metal foils, laser beam welding is the state-of-the-art technology. Current challenges include process instabilities at higher welding speeds, such as the humping effect, which can cause weld seam imperfections. Therefore, applying sensors for laser beam welding is a promising approach to monitor the welding process. AISI 316L foils were welded within the scope of this work with various process parameters using an adjustable ring mode laser beam source. Additionally, an optical microphone was used as a process monitoring system. By applying different parameter settings and due to the introduction of artificial faults, weld seam defects, such as a burn-through or a gap, were induced. After utilizing a noise reduction algorithm for the acoustic signals, numerous features in the time and frequency domain were extracted, with which multiple machine learning algorithms were trained and compared concerning their performance. A light gradient boosting machine was identified as a suitable machine learning model for the weld seam classification. Finally, a hyperparameter tuning was conducted, which resulted in a cross-validation accuracy of 94.78 %, depending on the quality categories considered.

Acoustic Process Monitoring During the Laser Beam Welding of Stainless-Steel Foils Using an Adjustable Ring Mode Laser Beam Source

In this paper, the necessity and theoretical analysis for Nanosecond-Scale Temperature Sensing Technology during Flat-Top Nanosecond Green Laser Annealing Process of Semiconductor Si-Wafer is overviewed. When a 532nm laser pulse with 10 ns or less pulse duration and several 100s mJ pulse energy is irradiated on the Si-wafer chip surface, the surface and internal temperature inside the chip is increased to several 100s or thousands quickly and cooled down during the next several 100s nanoseconds. The fastest commercial temperature sensor based on IR energy sensing has 40 us response time at which time the cooling process was already finished. So, the annealing process using 10 ns pulse laser annealing needs a proper method of ultrafast temperature measurement technology to understand the relationship between heated temperature and annealing quality which can make an impact on semiconductor chip performance. To resolve this issue, two-wavelength temperature measurement technology using fiber-guided sensing is selected among several technologies which is analyzed to know re-emission energy distribution from the Si-Chip and the captured energy into sensing fiber. Then, a proper focusing lens or lens set with optimum entrance pupil size to enhance the captured energy is determined. Then, a prototype setup for this two-tone temperature measurement is prepared and its performance is tried to compare with the results using a fast commercial temperature sensor.

Analysis of Nanosecond-Scale Temperature Sensing Technology for Flat-Top Nanosecond Green Laser Annealing Process of Semiconductor Si Wafers

Chromatic dispersion is a wavelength dependence of a group velocity of an optical fiber, and is an important fiber characteristic in fabricating pulse fiber lasers because it affects spectrum and pulse width. One of the chromatic dispersion measurement methods is a phase shift technique, which measures a relative phase shift between intensity-modulated lasers with different wavelengths. A disadvantage of this measurement method is that fiber lengths of several hundred meters or more are required to obtain high time resolution. Therefore, specialty fiber with short production lengths and amplification fiber that absorbs light of a specific wavelength, used for pulse fiber lasers, is difficult to measure with the method.

This study aims to develop a chromatic dispersion measurement method that can evaluate specialty fiber and amplification fiber using a short fiber under test of a few meters. The measurement light source used is a broadband light of high brightness and fiber optics that we developed. The feature of this study is that the fiber under test constitutes a Fabry-Perot resonator using the Fresnel reflections at both endfaces of the fiber. Enables measurement with the short fiber under test because it is measured from a standing wave of the resonator. The wavelength dependence of reflection characteristics from the standing wave is measured to obtain a relative group delay. Chromatic dispersion can be obtained by measuring the group delay difference at different wavelengths. Also, the fiber under test is the resonator, therefore measurement can be done without connectors and end face polishing.

Development of Wavelength Dispersion Measurement Method Using Fresnel Reflection of Fiber Under Test at Both End Faces

Laser welding is widely used in the automotive industry to join various materials due to its advantages of minimal thermal deformation and high productivity, applied in different joint

configurations, such as T-fillet and single-lap. The tensile properties of these joints are crucial for the stability of vehicle bodies, prompting research into both experimental and analytical evaluations. In particular, to experimentally evaluate the tensile properties of single-lap joints, a load cell-based force and crosshead displacement are generally used. However, the reliability of crosshead displacement data is affected by machine compliance and the specimen's dimensions, resulting in low reliability of displacement-related tensile properties such as structural stiffness. This can lead to discrepancies between experimental results and numerical analysis, which are critical for evaluating vehicle stability. Therefore, this study introduces a novel numerical modeling method for predicting structural stiffness using crosshead displacement during tensile testing of single-lap joints. Additionally, it presents modeling techniques to enhance the computational efficiency of the numerical model. Laser welding was performed on two types of materials, SPFC 590 and A6061, to make single-lap joint specimens. To evaluate the structural stiffness of these specimens, lap-shear tensile test was conducted. A three-dimensional numerical model based on ABAQUS software was developed, and a modeling method involving the application of an elastic modulus in the numerical model was proposed to enhance the correlation with the structural stiffness derived from lap-shear tensile test. Furthermore, modeling techniques such as optimizing mesh size and element type were suggested to enhance the computational efficiency.

A study on numerical modeling method for predicting structural stiffness using crosshead displacement in laser welded joints

Busbar welds play a pivotal role in battery pack assembly, as their quality significantly impacts the structural integrity, electrical conductivity, and thermal efficiency of the battery pack. Current in-line quality evaluation methods encompass diverse techniques, including resistance measurement, thermographic imaging for fusion area assessment, machine vision for weld surface scanning, and monitoring of spectral line intensities during the welding process. This research delves into the efficacy of several approaches across various production scenarios, considering the inherent variations in the production processes. Typical variations in laser power, gap condition, laser focus condition, surface contamination, weld location etc are considered and result in welds with different qualities. Process spectrum, weld surface morphology and resistance measurement data are meticulously analyzed by correlating them with joint strength derived from tensile testing. Porosity distributions characterized by X-ray are used for quality evaluation. The study reveals that weld surface morphology from machine vision and spectral line intensity data exhibit strong correlations with process variations and weld strength. Conversely, resistance data proves to be less sensitive to process changes and does not correlate well with weld strength and porosity levels. In summarizing the findings, this study offers recommendations on effective in-line inspection for ensuring the quality of busbar welds in production environments.

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Double-Pulse Laser Peening as a Surface Enhancement Technology

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